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Inorganic syntheses. Volume 35
- Available as
- Online
- Summary
-
The Inorganic Syntheses series provides all users of inorganic substances with detailed and foolproof procedures for the preparation of important and timely compounds.Includes complete, up-to-date ...
The Inorganic Syntheses series provides all users of inorganic substances with detailed and foolproof procedures for the preparation of important and timely compounds.Includes complete, up-to-date procedures involving important inorganic substancesContains subject, contributor, and formula indexes
Details
- Creator
- editor-in-chief Thomas B. Rauchfuss
- Format
- Books
- Language
- English
- Contributors
- Publication
-
- 1st ed
- Hoboken, NJ : Wiley, 2010
- Physical Details
-
- 1 online resource (221 p.)
- ISBNs
- 0470651563, 9780471682554, 9786612773068, 0471682551, 0470651547, 1282773062, 9780470651568
- OCLC
- ocn669165465, ocn813232516
- Description based upon print version of record.
- Includes bibliographical references and index.
- English
- INORGANIC SYNTHESES; PREFACE; CONTRIBUTORS; DEDICATION; NOTICE TO CONTRIBUTORS AND CHECKERS; TOXIC SUBSTANCES AND LABORATORY HAZARDS; CONTENTS; Chapter One COMPLEXES OF BULKY β-DIKETIMINATE LIGANDS; 1. INTRODUCTION; 2. β-DIKETIMINATE PRECURSORS HLMe,Me3 and TlLMe,Me3 (LMe,Me3 = 2,4-BIS-(MESITYLIMIDO)PENTYL); A. 2,4-BIS-(MESITYLIMIDO)PENTANE (HLMe,Me3); B. THALLIUM 2,4-BIS-(MESITYLIMIDO)PENTYL (TlLMe,Me3); 3. β-DIKETIMINATE PRECURSORS LMe,iPr2H, [LMe,iPr2Li]x,and [LtBu,iPr2K]x (LMe,iPr2=2,4-BIS-(2,6-DIISOPROPYLPHENYLIMIDO)PENTYL
- LtBu,iPr2=2,2,6,6-TETRAMETHYL-3,5-BIS-(2,6-DIISOPROPYLPHENYLIMIDO)HEPTYL)A. 2,4-BIS-(2,6-DIISOPROPYLPHENYLIMIDO)PENTANE (LMe,iPr2H); B. LITHIUM 2,4-BIS-(2,6-DIISOPROPYLPHENYLIMIDO)PENTYL([LMe,iPr2Li]x); C. POTASSIUM 2,2,6,6-TETRAMETHYL-3,5-BIS-(2,6-DIISOPROPYLPHENYLIMIDO)HEPTYL ([LtBu,iPr2K]x); 4. β-DIKETIMINATE PRECURSORS LtBu,iPr2H ANDLtBu,iPr2Li(THF) (LtBu,iPr2=2,2,6,6-TETRAMETHYL-3,5-BIS-(2,6-DIISOPROPYLPHENYLIMIDO)HEPTYL); A. N-PIVALOYL-2,6-DIISOPROPYLANILIDE (DIPPNHC(O)tBu); B. DIPPN=C(Cl)tBu; C. DIPPN=C(Me)tBu
- D. 2,2,6,6-TETRAMETHYL-3,5-BIS-(2,6-DIISOPROPYLPHENYLIMIDO)HEPTANE([DIPPN=C(tBu)]2CH2, LtBu,iPrH)E. LITHIUM 2,2,6,6-TETRAMETHYL-3,5-BIS-(2,6-DIISOPROPYLPHENYLIMIDO)HEPTYL (LtBu,iPr2Li, THFADDUCT); 5. SCANDIUM TRICHLORIDE TRIS(TETRAHYDROFURAN)AND β-DIKETIMINATE-SUPPORTED SCANDIUMCHLORIDE COMPLEXES; A. SCANDIUM TRICHLORIDE TRIS(TETRAHYDROFURAN),ScCl3(THF)3; B. SCANDIUM 2,4-BIS-(2,6-DIISOPROPYLPHENYLIMIDO)PENTYLDICHLORIDE TETRAHYDROFURAN, (LMe,iPr2)ScCl2(THF); C. SCANDIUM 2,2,6,6-TETRAMETHYL-3,5-BIS-(2,6-DIISOPROPYLPHENYLIMIDO)HEPTYL DICHLORIDE,(LtBu,iPr2)ScCl2
- 6. β-DIKETIMINATE-SUPPORTED TITANIUM ANDVANADIUM DICHLORIDE COMPLEXESA. SYNTHESIS OF (LMe,iPr2)TiCl2(THF); B. SYNTHESIS OF (LtBu,iPr2)TiCl2; C. SYNTHESIS OF (LMe,iPr2)VCl2; 7. β-DIKETIMINATE-SUPPORTED VANADIUM AND CHROMIUM CHLORIDE COMPLEXES; A. SYNTHESIS OF LMe,Me2VCl2; B. SYNTHESIS OF LMe,Me2CrCl2(THF)2; 8. β-DIKETIMINATE-SUPPORTED MANGANESE AND ZINC COMPLEXES; A. LMe,iPr2MnI(THF); B. THE THF-FREE DIMER (LMe,iPr2MnI)2; C. LMe,iPr2ZnCl2Li(OEt2)2; 9. IRON 2,4-BIS-(2,6-DIISOPROPYLPHENYLIMIDO)PENTYL CHLORIDE (LMe,iPr2FeCl)
- 10. IRON 2,2,6,6-TETRAMETHYL-3,5-BIS-(2,6- DIISOPROPYLPHENYLIMIDO)HEPTYL CHLORIDE (LtBu,iPr2FeCl)11. COBALT 2,2,6,6-TETRAMETHYL-3,5-BIS-(2,6- DIISOPROPYLPHENYLIMIDO)HEPTYL CHLORIDE (LtBu,iPr2CoCl); 12. β-DIKETIMINATE-SUPPORTED NICKEL(II) AND NICKEL(I) COMPLEXES OF LME,ME3 (LME,ME3=2,4-BIS- (MESITYLIMIDO)PENTYL); A. LMe,Me3NiI(2,4-LUTIDINE); B. LMe,Me3Ni(2,4-LUTIDINE); 13. NICKEL 2,4-BIS-(2,6-DIISOPROPYLPHENYLIMIDO) PENTYL CHLORIDE DIMER, [LMe,iPr2Ni(μ-Cl)]2; 14. BIS[COPPER 2,4-BIS-(2,4,6-TRIMETHYLPHENYLIMIDO) PENTYL] TOLUENE, (LMe,Me3Cu)2(μ-η2:η2-C7H8); A. COPPER tert-BUTOXIDE
- B. BIS[COPPER 2,4-BIS-(2,4,6-TRIMETHYLPHENYLIMIDO) PENTYL] TOLUENE